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Experiments in Organic Chemistry

Experiments in Organic Chemistry - 3rd edition

ISBN13: 978-0898923117

Cover of Experiments in Organic Chemistry 3RD 05 (ISBN 978-0898923117)
ISBN13: 978-0898923117
ISBN10: 0898923115
Cover type:
Edition/Copyright: 3RD 05
Publisher: Contemporary Publishing Company of Raleigh
Published: 2005
International: No

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Experiments in Organic Chemistry - 3RD 05 edition

ISBN13: 978-0898923117

Richard K. Hill

ISBN13: 978-0898923117
ISBN10: 0898923115
Cover type:
Edition/Copyright: 3RD 05
Publisher: Contemporary Publishing Company of Raleigh

Published: 2005
International: No
Summary

Originally written for the University of Georgia Organic Chemistry labs, this manual has been expanded and now has over 50 adoptions throughout the country. Most of the lab manual's experiments are small-scale, using 1-5 g of starting materials, and a large majority are also designed for microscale laboratories, using 50-200 mg of reagents, making this manual suitable for both standard or microscale operations.

Table of Contents

Prefece and Acknowledgments

GENERAL INFORMATION

G1- Safety and Waste Disposal
G2- Laboratory Notebook and Lab Reports
G3- Glassware

FUNDAMENTAL LABORATORY TECHNIQUES

T1- General techniques
T2- Recrystallization
T3- Melting Points
T4- Distillation
T5- Extraction
T6- Drying and Drying Agents
T7- Thin-layer Chromatography
T8- Gas Chromatography
T9- Calculation of Percent Yield

EXPERIMENTS

E1- Purification of an Unknown Solid by Recrystallization and Identification by Melting Point
E2- Distillation
E3- Thin-layer Chromatography
E4- Extraction of Organic Compounds from Natural Sources
E5- Dehydration of Alcohols
E6- Preparation of Diphenylacetylene
E7- The Diels-Alder Reaction
E8- Preparation and Substitution Reactions of Alkyl Halides
E9- Electrophilic Aromatic Substitution: Nitration
E10- Friedel-Crafts Reactions
E11- Oxidation of Alcohols: Preparation of Camphor
E12- The Aldol Condensation: Preparation of Dibenzalacetone
E13- The Knoevenagel Condensation: Preparation of Ethel 3-Coumarincarboxylate
E14- Identification of an Unknown Aldehyde or Ketone
E15- The Wittig Reaction: Preparation of 1,4-Diphenyl-1,3-butadiene, and E-9-(2-Phenylethenyl)anthracene
E16- The Grignard Reaction: Preparation of Triphenylmethanol & Benzoic Acid
E17- The Williamson Ether Synthesis: Preparation of an Aryloxyacetic Acid from Cresol
E18- Fischer Esterification
E19- Preparation of Aspirin
E20- Amides
E21- Formation and Reactions of Cyclic Anhydrides
E22- Oxidative Coupling of 2-Naphthol
E23- Reactions of Aryl Diazonium Salts
E24- Carbohydrates
E25- Sodium Borohydride Reduction of Benzil and Determination of Acetonide Stereochemistry by H NMR
E26- Hydrogenation of Olive Oil

MYSTERY REACTIONS
APPENDIX

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