Steps in Chemical Analysis SI Units and Prefixes Conversion Between Units Chemical Concentrations Preparing Solutions
2. Tools of the Trade
Safety with Chemicals and Waste Your Lab Notebook The Analytical Balance Burets Volumetric Flasks Pipets and Syringes Filtration Drying Calibration of Volumetric Glassware Methods of Sample Preparation
3. Math Toolkit
Significant Figures Significant Figures in Arithmetic Types of Error Propagation of Uncertainty Introducing Spreadsheets Spreadsheet + Graph = Power
The Gaussian Distribution Student's t Q Test for Bad Data Finding the "Best" Straight Line Constructing a Calibration Curve A Spreadsheet for Least Squares
5. A Skirmish with Equilibrium
The Equilibrium Constant Solubility Product What Are Acids and Bases? The Relation Between [H+], [OH-], and pH Strengths of Acids and Bases
6. Good Titrations
Principles of Volumetric Analysis Titration Calculations Titration of a Mixture Chemistry in a Fishtank Titrations Involving Silver Ion
7. Let There Be Light
Properties of Light Absorption of Light The Spectrophotometer
Using Beer's Law Spectrophotometric Titrations Luminescence Immunoassays
9. Monoprotic Acid-Base Equilibria
Strong Acids and Bases Weak Acids and Bases Weak-Acid Equilibrium Weak-Base Equilibrium Fractional Composition Equations
What You Mix Is What You Get The Henderson-Hasselbach Equation A Buffer in Action Preparing Buffers Buffer Capacity How Indicators Work
11. Acid-Base Titrations
Titration of Strong Acid with Strong Base Titration of Weak Acid with Strong Base Titration of Weak Base with Strong Acid Finding the End Point Practical Notes Kjeldahl Nitrogen Analysis Putting Your Spreadsheet to Work
12. Polyprotic Acids and Bases
Amino Acids Are Polyprotic Finding the pH in Diprotic Systems Which is the Principal Species? Titrations in Polyprotic Systems
13. Electrode Potentials
Redox Chemistry and Electricity Galvanic Cells Standard Potentials The Nernst Equation E° and the Equilibrium Constant Reference Electrodes
14. Electrode Measurements
The Silver Indicator Electrode What Is a Junction Potential? How Ion-Selective Electrodes Work pH Measurement with a Glass Electrode Ion-Selective Electrodes
15. EDTA and Iodine Titrations
Metal-Chelate Complexes EDTA Metal Ion Indicators EDTA Titration Techniques Titrations Involving Iodine
16. Principles of Chromatography
What Is Chromatography? How We Describe a Chromatogram Why Do Bands Spread? Chemical Analysis by Chromatography Internal Standards
17. Gas and Liquid Chromatography
Gas Chromatography Classical Liquid Chromatography High-Performance Liquid Chromatography
18. Chromatographic Methods and Capillary Electrophoresis
Ion-Exchange Chromatography Ion Chromatography Molecular Exclusion Chromatography Affinity Chromatography What Is Capillary Electrophoresis? How Capillary Electrophoresis Works Types of Capillary Electrophoresis
19. Gravimetric and Combustion Analysis
An Example of Gravimetric Analysis Precipitation Examples of Gravimetric Calculations Combustion Analysis
20. Atomic Spectroscopy
What Is Atomic Spectroscopy? Atomization: Flames, Furnaces, and Plasmas How Temperature Affects Atomic Spectroscopy Instrumentation Interference Quantitative Analysis by Standard Addition
Penny Statistics Statistical Evaluation of Acid-Base Indicators Calibration of Volumetric Glassware Gravimetric Determination of Calcium as CaC2O4 * H20 Gravimetric Measurement of Phosphorus in Plant Food Preparing Standard Acid and Base Analysis of a Mixture of Carbonate and Bicarbonate Kjeldahl Nitrogen Analysis Using a pH Electrode for an Acid-Base Titration EDTA Titration of Ca2+ and Mg2+ in Natural Waters Synthesis and Analysis of Ammonium Decavanadate Iodimetric Titration of Vitamin C Potentiometric Halide Titration with AG+ Spectrophotometric Nitrite Determination of Aquarium Water Measuring Ammonia in a Fishtank with an Ion-Selective Electrode Spectrophotometric Determination of Iron in Dietary Tablets Microscale Spectrophotometric Measurement of Iron in Foods by Standard Addition Properties of an Ion-Exchange Resin Using an Internal Standard in Gas Chromatography or High-Performance Liquid Chromatography Analysis of Sulfur in Coal by Ion Chromatography Measuring Carbon Monoxide in Automobile Exhaust by Gas Chromatography Amino Acid Analysis by Capillary Electrophoresis
Glossary Appendix A: Solubility Products
Appendix B: Acid Dissociation Constants
Appendix C: Standard Reduction Potentials
Appendix D: Oxidation Numbers and Balancing Redox Equations
Solutions to "Ask Yourself" Questions
Answers to Problems
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