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Introduction to Organic Laboratory Techniques : A Small Scale Approach

Introduction to Organic Laboratory Techniques : A Small Scale Approach - 98 edition

ISBN13: 978-0030245190

Cover of Introduction to Organic Laboratory Techniques : A Small Scale Approach 98 (ISBN 978-0030245190)
ISBN13: 978-0030245190
ISBN10: 0030245192
Cover type:
Edition/Copyright: 98
Publisher: Saunders College Division
Published: 1998
International: No

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Introduction to Organic Laboratory Techniques : A Small Scale Approach - 98 edition

ISBN13: 978-0030245190

Donald L. Pavia, George S. Kriz, Gary M. Lampman and Randall G. Engel

ISBN13: 978-0030245190
ISBN10: 0030245192
Cover type:
Edition/Copyright: 98
Publisher: Saunders College Division

Published: 1998
International: No
Summary

In this laboratory textbook for students of organic chemistry, experiments are designed to utilize standard-scale (''macroscale'') glassware and equipment but with smaller amounts of chemicals and reagents. The textbook features a large number of traditional organic reactions and syntheses, as well as the isolation of natural products and experiments with a biological or health sciences focus. The organization of the text is based on essays and topics of current interest. Contains a comprehensive treatment of laboratory techniques including both small-scale and some microscale methods.

Table of Contents

Part One: Preparations and Reactions of Organic Compounds

1. Isolation of the Active Ingredient in an Analgesic Drug
2. Acetylsalicylic Acid
3. Acetanilide
4. Acetaminophen
5. Isolation of Caffeine
6. TLC Analysis of Analgesic Drugs
7. Ethanol from Sucrose
8. Isopentyl Acetate (Banana Oil)
9. Preparation of a C-4 or C-5 Acetate Ester
10. Methyl Salicylate (Oil of Wintergreen)
11. Hydrolysis of Methyl Salicylate
12. Analysis of Fats and Oils by Gas Chromatography
13. Methyl Stearate from Methyl Oleate
14. Preparation of Soap
15. Preparation of a Detergent
16. N, N-Diethyl-m-toluamide: The Insect Repellent 'OFF'
17. Gas Chromatographic Analysis of Gasolines
18. Isolation of Essential Oils from Allspice, Cloves, Cumin, Caraway, Cinnamon, or Fennel
19. Thin-Layer Chromatography for Monitoring the Oxidation of Borneol to Camphor
20. An Oxidation-Reduction Scheme: Borneol, Camphor, Isoborneol
21. Spearmint and Caraway Oil: (-)- and (+)-Carvones
22. Reactivities of Some Alkyl Halides
23. Synthesis of n-Butyl Bromide and t-Pentyl Chloride
24. Nucleophilic Substitution Reactions: Competing Nucleophiles
25. Hydrolysis of Some Alkyl Chlorides
26. Chromic Acid Oxidation of Alcohols
27. 4-Methylcyclohexene
28. Phase Transfer Catalysis: Addition of Dichlorocarbene to Cyclohexene
29. Markovnikov and anti-Markovnikov Hydration of 1-Methylcyclohexene
30. Triphenylmethanol and Benzoic Acid
31. Carbonation of an Unknown Aromatic Halide
32. The Preparation of Pinacol and the Pinacol Rearrangement
33. Nitration of Methyl Benzoate
34. Relative Reactivities of Several Aromatic Compounds
35. Friedel-Crafts Acylation
36. Methyl Orange
37. Dyes, Fabrics, and Dyeing
38. Chromatography of Some Dye Mixtures
39. Isolation of Carotenoid Pigments from Spinach
40. Coenzyme Synthesis of Benzoin
41. Benzil
42. Benzilic Acid
43. Sulfa Drugs: Preparation of Sulfanilamide
44. p-Aminobenzoic Acid
45. Benzocaine
46. Tetraphenylcyclopentadienone
47. Enamine Reactions: 2-Acetylcyclohexanone
48. The Aldol Condensation: Preparation of Benzalacetophenones (Chalcones)
49. Preparation of an a, B-Unsaturated Ketone via Michael and Aldol Condensation Reactions
50. An Introduction to Molecular Modeling
51. The Diels-Alder Reaction of Cyclopentadiene with Maleic Anhydride
52. Benzyne Formation and the Diels-Alder Reaction: Preparation of 1,2,3,4 Tetraphenylnaphthalene
53. Photoreduction of Benzophenone and Rearrangement of Benzpinacol to Benzopinacolone
54. Luminol
55.cis,trans-, and trans,trans-1,4-Diphenyl-1,3-butadiene
56. Preparation of Polymers: Polyester, Nylon, and Polystyrene
57. Identification of Unknowns
58. Carbohydrates
59. Analysis of a Diet Soft Drink by HPLC
60. Isolation of Casein and Lactose from Milk
61. Mutarotation of Lactose
62. Resolution of (+)-a-Phenylethylamine and Determination of Optical Purity
63. Chiral Reduction of Ethyl Acetoacetate: Optical Purity Determination Using a Chiral Shift Reagent
64. Esterification Reactions of Vanillin: The Use of NMR to Solve a Structure Proof Problem
65. The Fatty Acids: An Exercise in Molecular Modeling

Part Two: The Techniques

1. Measurement of Volume and Weight
2. Heating and Cooling Methods
3. Reaction Methods
4. Filtration
5. Crystallization: Purification of Solids
6. Physical Constants: Melting Points, Boiling Points, Density
7. Extractions, Separations, and Drying Agents
8. Simple Distillation
9. Vacuum Distillation, Manometers
10. Fractional Distillation, Azeotropes
11. Steam Distillation
12. Column Chromatography
13. High-Performance Liquid Chromatography
14. Thin-Layer Chromatography
15. Gas Chromatography
16. Sublimation
17. Polarimetry
18. Refractometry
19. Preparation of Samples for Spectroscopy
20. Guide to the Chemical Literature

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Cover of Introduction to Organic Laboratory Techniques : A Small Scale Approach 2nd edition

Introduction to Organic Laboratory Techniques : A Small Scale Approach - 2nd edition

ISBN13: 978-0534408336
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