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Measurement and Synthesis in the Chemistry Laboratory

Measurement and Synthesis in the Chemistry Laboratory - 92 edition

ISBN13: 978-0023598357

Cover of Measurement and Synthesis in the Chemistry Laboratory 92 (ISBN 978-0023598357)
ISBN13: 978-0023598357
ISBN10: 0023598352
Cover type:
Edition/Copyright: 92
Publisher: Macmillan Publishing Co.
Published: 1992
International: No

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Measurement and Synthesis in the Chemistry Laboratory - 92 edition

ISBN13: 978-0023598357

Larry Peck

ISBN13: 978-0023598357
ISBN10: 0023598352
Cover type:
Edition/Copyright: 92
Publisher: Macmillan Publishing Co.

Published: 1992
International: No
Summary

This laboratory manual contains thirty-three chemistry experiments designed to introduce readers/students to the world of chemistry and to teach them general and specific laboratory skills. Using a variety of techniques and substances that are familiar in everyday life -- they engage readers/students in such activities as synthesizing a substance, finding the composition of an ore sample, checking the effectiveness of an antacid, etc. Each well-structured, illustrated lab features background information, a theoretical framework for the experiment, necessary mathematical derivations, a summary and checklist of general laboratory activities, step-by-step procedures, safety precautions, and pre- and post-lab exercises and report forms. Several appendices cover common laboratory operations and statistical treatment of data.

Table of Contents

1. Precision - Accuracy - Calibration.
2. Truth in Labeling - A Balance Experiment.
3. Density Determinations.
4. Chemical Economics.
5. Alum from Aluminum Beverage Cans.
6. Growing Alum Crystals.
7. The Manufacturing of Soap.
8. From Soap to Fatty Acid.
9. Detecting Iron, Copper and Lead in Ores.
10. Copper(II) and Algae.
11. Tetraamminecopper(II) Sulfate.
12. Formula Weight of a Fatty Acid.
13. Alka-Seltzer®® and a Little Gas.
14. Molecular Mass of a Volatile Hydrocarbon.
15. Molecular Masses of Pharmaceutical Chemicals.
16. Heat Storage for Solar Heating.
17. Rayon: A Valuable Polymer.
18. Analysis of an Unknown Oxalate Sample.
19. Determination of Iron in Pyrites.
20. The Kinetics of the Decomposition of Hydrogen Peroxide.
21. Some Commercial Antacids.
22. Determination of an Ionization Constant.
23. The NH3/NH4Cl Buffer System.
24. Enthalpy of Ionization of Acetic Acid.
25. Electrochemical Galvanic Cells.
26. A Cobalt Complex.
27. Calcium in Natural Materials.
28. Spectrophotometric Determination of Glucose.
29. Composition of an Fe(III)-SCN Complex.
30. Colorimetric Determination of Copper as Cu(ethylenediamine)2^2+.
31. Models for Organic Compounds.
32. Identification of OrganicCompounds.
33. Amyl Acetate, a Natural Flavoring Agent.
Appendix A. Weighing to the Nearest 0.01 Gram.
Appendix B. Weighing with an Analytical Balance.
Appendix C. Transfer of Solids or Liquids.
Appendix D. Delivering Measured Volumes of Liquids from a Buret.
Appendix E. Use of a Laboratory Centrifuge.
Appendix F. Vacuum Filtration.
Appendix G. Inserting Glass Tubing into Stoppers.
Appendix H. Precision, Accuracy, Significant Figures

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