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Microscale and Macroscale Techniques in the Organic Laboratory

Microscale and Macroscale Techniques in the Organic Laboratory - 02 edition

ISBN13: 978-0030343117

Cover of Microscale and Macroscale Techniques in the Organic Laboratory 02 (ISBN 978-0030343117)
ISBN13: 978-0030343117
ISBN10: 0030343119
Cover type: Hardback
Edition/Copyright: 02
Publisher: Harcourt Brace or Harcourt Press
Published: 2002
International: No

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Microscale and Macroscale Techniques in the Organic Laboratory - 02 edition

ISBN13: 978-0030343117

Donald L. Pavia

ISBN13: 978-0030343117
ISBN10: 0030343119
Cover type: Hardback
Edition/Copyright: 02
Publisher: Harcourt Brace or Harcourt Press

Published: 2002
International: No
Summary

The well-known and tested organic chemistry laboratory techniques of the two best-selling organic chemistry lab manuals: Introduction to Organic Laboratory Techniques: A Small Scale Approach and Introduction to Organic Laboratory Techniques: A Small Scale Approach, 3/e are now assembled in one textbook. Professors can use any experiments alongside Microscale and Macroscale Techniques in the Organic Laboratory. Experiments can be selected and assembled from the two Pavia organic chemistry lab manuals, from professors' homegrown labs, or even competing texts. The 375 page, hardcover book serves as a reference for all students of organic chemistry. With clearly written prose and accurately drawn diagrams, students can feel confident setting up and running organic labs.

Table of Contents

1. Laboratory Safety.
2. Advance Preparation and Laboratory Records.
3. Laboratory Glassware.
4. How to Find Data for Your Compound: Handbooks and Catalogues.
5. Measurement of Volume and Weight.
6. Heating and Cooling Methods.
7. Reaction Methods.
8. Filtration.
9. Physical Constants of Solids: The Melting Point.
10. Solubility.
11. Crystallization: Purification of Solids.
12. Extractions, Separations, and Drying Agents.
13. Physical Constants of Liquids: Boiling Point and Density.
14. Simple Distillation.
15. Fractional Distillation; Azeotropes.
16. Vacuum Distillation; Manometers.
17. Sublimation.
18. Steam Distillation.
19. Column Chromatography.
20. Thin-Layer Chromatography.
21. High-Performance Liquid Chromatography (HPLC).
22. Gas Chromatography.
23. Polarimetry.
24. Refractometry.
25. Infrared Spectroscopy.
26. Nuclear Magnetic Resonance Spectroscopy (Proton NMR).
27. Carbon-13 Nuclear Magnetic Resonance Spectroscopy.
28. Mass Spectrometry.
29. Computational Chemistry.
30. Guide to the Chemical Literature.

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