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Organic Chemistry Laboratory : Standard and Microscale Experiments

Organic Chemistry Laboratory : Standard and Microscale Experiments - 3rd edition

ISBN13: 978-0030292729

Cover of Organic Chemistry Laboratory : Standard and Microscale Experiments 3RD 01 (ISBN 978-0030292729)
ISBN13: 978-0030292729
ISBN10: 0030292727
Cover type: Hardback
Edition/Copyright: 3RD 01
Publisher: Harcourt Brace or Harcourt Press
Published: 2001
International: No

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Organic Chemistry Laboratory : Standard and Microscale Experiments - 3RD 01 edition

ISBN13: 978-0030292729

Charles E. Bell, Allen K. Clark, Douglass F. Taber and Oscar D. Rodig

ISBN13: 978-0030292729
ISBN10: 0030292727
Cover type: Hardback
Edition/Copyright: 3RD 01
Publisher: Harcourt Brace or Harcourt Press

Published: 2001
International: No
Summary

The new edition continues to offer a wide variety of organic lab experiments for both standard and microscale formats and features unusually strong coverage of spectroscopy.

Author Bio

Bell, Charles E. : Old Dominion University


Taber, Douglas : University of Delaware


Clark, Allen K. : Old Dominion University

Table of Contents

1. Introduction.
2. Melting Points.
3. Recrystallization.
4. Extraction.
5. Distillation.
6. Gas Chromatography.
7. Column Chromatography.
8. Thin Layer Chromatography.
9. High Performance Liquid Chromatography.
10. Steam Distillation of Essential Oils.
11. Infrared Absorption Spectroscopy.
12. Spectroscopic Structure Determination: A Lifelong Quest.
13. Proton Nuclear Magnetic Resonance.
14. Advanced Structure Determination.
15. The Literature of Organic Chemistry.
16. Properties of Hydrocarbons.
17. Nucleophylic Substitution of Alkyl Halides.
18. Properties of Alcohols.
19. The Grignard Reaction.
20. Dehydration of Alcohols.
21. Oxidation and Reduction.
22. Aldehydes and Ketones.
23. Determination of pK(a): Effects of Substituents on Acidity.
24.Carboxylic Acid Mini-unknown.
25. Esterification and Saponification: Effect of Substituents on Reactivity.
26. Friedel-Crafts Alkylation and Acylation.
27. Aromatic Nitration.
28. Aromatic Nucleophilic Substitution.
29. Properties of Amines.
30. Chemiluminescence.
31. Photodimerization of Benzophenone.
32. The Diels-Alder Reaction.
33. Phase Transfer Catalysis.
34. Derivatives of Caroboxylic Acids: Synthesis of a Plant Hormone.
35. Synthesis of Coumarin.
36. Benzyne.
37. Heterocyclic Syntheses: Pyrimidines, Pyridones, Isoxazoles, Quinolines, and Indoles.
38. Heterocyclic Synthesis: Phenytoin.
39. Synthesis of Sulfanilamide.
40. Resolution of a-Phenylethylamine.
41. Chemistry of Sugars.
42. Acid-Catalyzed and Enzyme-Catalyzed Hydrolosis of Polysaccharides.
43. Analysis of Fats and Oils.
44. Synthetic Organic Polymers.
45. Dyes and Dyeing.
46. Qualitative Organic Analysis.
Appendix A: Selected Atomic Weights.
Appendix B: Common Acids and Bases.
Appendix C: Common Organic Liquids.
Appendix D: Representative Calculations.

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