ISBN13: 978-0070570740

ISBN10: 0070570744

Cover type:

Edition/Copyright: 6TH 96

Publisher: McGraw-Hill Publishing Company

Published: 1996

International: No

ISBN10: 0070570744

Cover type:

Edition/Copyright: 6TH 96

Publisher: McGraw-Hill Publishing Company

Published: 1996

International: No

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This best-selling comprehensive manual is for a junior/senior level laboratory course in physical chemistry. Forty-eight labs are included with theoretical notes, safety recommendation and computer applications. Significant updating is done to the treatment of experimental data and the use of computers.

Author Bio

**Shoemaker, David P. :**

Garland, Carl W. : Massachusetts Institute of Technology

Nibler, Joseph W. : Oregon State University

**1 Introduction**

Organization of the Book, Preparation for an Experiment, Execution of an Experiment, Safety, Recording of Experimental Data, Literature Work, Reports, Sample Reports, Special Projects

**2 Treatments of Experimental Data: **

A. Calculations and Presentation of Data: Significant Figures, Precision of Calculations, Analytical Methods, Numerical Methods, Graphs and Graphical Methods, Exercises;

B. Uncertainties in Data and Results: Errors, Rejection of Discordant Data, Statistical Treatment of Random Errors, Significance Testing, Propagation of Errors, Case History of an Error Evaluation, Fundamental Limitations on Instrumental Precision, Summary, Exercises

**3 Use of Computer Software: **

Word Processors, Spreadsheets, Symbolic Mathematics Programs, Quantum Mechanical Programs, Exercises

**4 Gases: **

Gas Thermometry, Joule-Thomson Effect, Heat Capacity Ratios for Gases

**5 Transport Properties of Gases: **

Kinetic Theory of Transport Phenomena, Viscosity of Gases, Diffusion of Gases

**6 Thermochemistry: Principles of Calorimetry: **

Heats of Combustion, Strain Energy of the Cyclopropane Ring, Heats of Ionic Reaction

**7 Solutions: **

Partial Molal Volume, Cryoscopic Determination of Molecular Weight, Freezing-Point Depression of Strong and Weak Electrolytes, Chemical Equilibrium in Solution

**8 Phase Equilibria: **

Vapor Pressure of a Pure Liquid, Binary Liquid-Vapor Phase Diagram, Binary Solid-Liquid Phase Diagram, Liquid-Vapor Coexistence Curve and the Critical Point

**9 Electrochemistry: **

Conductance of Solutions, Temperature Dependence of EMF, Activity Coefficients from Cell Measurements

**10 Chemical Kinetics, Method of Initial Rate: **

Iodine Clock, NMR Study of a Reversible Hydrolysis Reaction, Enzyme Kinetics: Inversion of Sucrose, Kinetics of the Decomposition of Benzenediazonium Ion, Gas-Phase Kinetics

**11 Surface Pheomena: **

Surface Tension of Solutions, Physical Adsorption of Gases

**12 Macromolecules: **

Osmotic Pressure, Alcohol, Helix-Coil Transition in Polypeptides

**13 Electric and Magnetic Properties: **

Dipole Moment of Polar Molecules in Solution, Dipole Moment of HCI Molecules in the Gas Phase, Magnetic Susceptibility, NMR Determination of Paramagnetic Susceptibility

**14 Spectroscopy: **

Absorption Spectrum of a Conjugated Dye, Infrared Spectroscopy: Vibrational Spectrum of SO2, Raman Spectroscopy: Vibrational Spectrum of CC14, Vibrational-Rotational Spectra of HC1 and DC1, Vibrational-Rotational Spectra of Acetylenes, Band Spectrum of Nitrogen, Absorption and Emission Spectra of Molecular Iodine, Electron Spin Resonance Spectroscopy, NMR Determination of Keto-Enol Equilibrium Constants, NMR Study of Gas Phase HC1-DBr Isotopic Exchange Reaction, Solid-State Lasers: Radiative Properties of Ruby Crystals

**15 Solids: **

Determination of Crystal Structure by X-Ray Diffraction, Single Crystal X-Ray Diffraction with the Buerger Precession Camera, Lattic Energy of Solid Argon, Statistical Thermodynamics of Iodine Sublimation

**16 Computer Interfacing: **

Introduction, Types of Information Handled, Hardware, Software, Computer Programmin, Interfacing with Experiments

**17 Electronic Devices and Measurements: **

Circuit Elements, Semiconductor Devices, Operational Amplifiers, Analog-to-digital Conversion, Digital Multimeters, Potentionmeter Circuits, Wheatstone Bridge Circuits, Capacitance Measurements

**18 Temperature: **

Temperature Scales, Triple-Point and Ice Point Cell, Thermometers, Temperature Control

**19 Vacuum Techniques: **

Introduction, Theoretical Background, Pumping Speed for a System, Desorption and Virtual Leaks, Pumps, Vacuum Gauges, Miscellaneous Vacuum Components, Design of Vacuum Compenents, Design of Vacuum Lines, Leak Detection, Safety Considerations

**20 Instruments: **

Balances, Barometer, Oscilloscope, pH Meter, Polarimeter, Radiation Counters, Recorders and Plotters, Refractometers, Signal-Average Devices, Spectroscopic Components, Spectroscopic Instruments, Timing Devices, Westphal Balance

**21 Miscellaneous Procedures: **

Volumetric Procedures, Purification Methods, Gas-Handling Procedures, Electrodes for Electrochemical Cells, Materials for Construction, Solders and Adhesives, Tubing Connections, Shopwork

**22 Least Squares Fitting Procedures: **

Introduction, Foundations of Least Squares, Weights, Rejection of Discordant Data, Goodness of Fit, Compersion of Models, Uncertainties in the Parameters Summary of Procedures, Sample Least-Squares, Calculation

**Appendixes **

A: Glossary of Symbols

B: International System of Units and Concentration Units

C: Safety, D: Literature Work

E: Research Journals

F: Numerical Methods of Analysis

G: Garomenter Corrections.

David P. Shoemaker, Carl W. Garland and Joseph W. Nibler

ISBN13: 978-0070570740ISBN10: 0070570744

Cover type:

Edition/Copyright: 6TH 96

Publisher: McGraw-Hill Publishing Company

Published: 1996

International: No

This best-selling comprehensive manual is for a junior/senior level laboratory course in physical chemistry. Forty-eight labs are included with theoretical notes, safety recommendation and computer applications. Significant updating is done to the treatment of experimental data and the use of computers.

Author Bio

**Shoemaker, David P. :**

Garland, Carl W. : Massachusetts Institute of Technology

Nibler, Joseph W. : Oregon State University

Table of Contents

**1 Introduction**

Organization of the Book, Preparation for an Experiment, Execution of an Experiment, Safety, Recording of Experimental Data, Literature Work, Reports, Sample Reports, Special Projects

**2 Treatments of Experimental Data: **

A. Calculations and Presentation of Data: Significant Figures, Precision of Calculations, Analytical Methods, Numerical Methods, Graphs and Graphical Methods, Exercises;

B. Uncertainties in Data and Results: Errors, Rejection of Discordant Data, Statistical Treatment of Random Errors, Significance Testing, Propagation of Errors, Case History of an Error Evaluation, Fundamental Limitations on Instrumental Precision, Summary, Exercises

**3 Use of Computer Software: **

Word Processors, Spreadsheets, Symbolic Mathematics Programs, Quantum Mechanical Programs, Exercises

**4 Gases: **

Gas Thermometry, Joule-Thomson Effect, Heat Capacity Ratios for Gases

**5 Transport Properties of Gases: **

Kinetic Theory of Transport Phenomena, Viscosity of Gases, Diffusion of Gases

**6 Thermochemistry: Principles of Calorimetry: **

Heats of Combustion, Strain Energy of the Cyclopropane Ring, Heats of Ionic Reaction

**7 Solutions: **

Partial Molal Volume, Cryoscopic Determination of Molecular Weight, Freezing-Point Depression of Strong and Weak Electrolytes, Chemical Equilibrium in Solution

**8 Phase Equilibria: **

Vapor Pressure of a Pure Liquid, Binary Liquid-Vapor Phase Diagram, Binary Solid-Liquid Phase Diagram, Liquid-Vapor Coexistence Curve and the Critical Point

**9 Electrochemistry: **

Conductance of Solutions, Temperature Dependence of EMF, Activity Coefficients from Cell Measurements

**10 Chemical Kinetics, Method of Initial Rate: **

Iodine Clock, NMR Study of a Reversible Hydrolysis Reaction, Enzyme Kinetics: Inversion of Sucrose, Kinetics of the Decomposition of Benzenediazonium Ion, Gas-Phase Kinetics

**11 Surface Pheomena: **

Surface Tension of Solutions, Physical Adsorption of Gases

**12 Macromolecules: **

Osmotic Pressure, Alcohol, Helix-Coil Transition in Polypeptides

**13 Electric and Magnetic Properties: **

Dipole Moment of Polar Molecules in Solution, Dipole Moment of HCI Molecules in the Gas Phase, Magnetic Susceptibility, NMR Determination of Paramagnetic Susceptibility

**14 Spectroscopy: **

Absorption Spectrum of a Conjugated Dye, Infrared Spectroscopy: Vibrational Spectrum of SO2, Raman Spectroscopy: Vibrational Spectrum of CC14, Vibrational-Rotational Spectra of HC1 and DC1, Vibrational-Rotational Spectra of Acetylenes, Band Spectrum of Nitrogen, Absorption and Emission Spectra of Molecular Iodine, Electron Spin Resonance Spectroscopy, NMR Determination of Keto-Enol Equilibrium Constants, NMR Study of Gas Phase HC1-DBr Isotopic Exchange Reaction, Solid-State Lasers: Radiative Properties of Ruby Crystals

**15 Solids: **

Determination of Crystal Structure by X-Ray Diffraction, Single Crystal X-Ray Diffraction with the Buerger Precession Camera, Lattic Energy of Solid Argon, Statistical Thermodynamics of Iodine Sublimation

**16 Computer Interfacing: **

Introduction, Types of Information Handled, Hardware, Software, Computer Programmin, Interfacing with Experiments

**17 Electronic Devices and Measurements: **

Circuit Elements, Semiconductor Devices, Operational Amplifiers, Analog-to-digital Conversion, Digital Multimeters, Potentionmeter Circuits, Wheatstone Bridge Circuits, Capacitance Measurements

**18 Temperature: **

Temperature Scales, Triple-Point and Ice Point Cell, Thermometers, Temperature Control

**19 Vacuum Techniques: **

Introduction, Theoretical Background, Pumping Speed for a System, Desorption and Virtual Leaks, Pumps, Vacuum Gauges, Miscellaneous Vacuum Components, Design of Vacuum Compenents, Design of Vacuum Lines, Leak Detection, Safety Considerations

**20 Instruments: **

Balances, Barometer, Oscilloscope, pH Meter, Polarimeter, Radiation Counters, Recorders and Plotters, Refractometers, Signal-Average Devices, Spectroscopic Components, Spectroscopic Instruments, Timing Devices, Westphal Balance

**21 Miscellaneous Procedures: **

Volumetric Procedures, Purification Methods, Gas-Handling Procedures, Electrodes for Electrochemical Cells, Materials for Construction, Solders and Adhesives, Tubing Connections, Shopwork

**22 Least Squares Fitting Procedures: **

Introduction, Foundations of Least Squares, Weights, Rejection of Discordant Data, Goodness of Fit, Compersion of Models, Uncertainties in the Parameters Summary of Procedures, Sample Least-Squares, Calculation

**Appendixes **

A: Glossary of Symbols

B: International System of Units and Concentration Units

C: Safety, D: Literature Work

E: Research Journals

F: Numerical Methods of Analysis

G: Garomenter Corrections.

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